HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → HCID 23381347, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | HCID 18173649 | HCID 18173649 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Product | HCID 23381347 | HCID 23381347 | — |
Reaction Steps
N-[4-(Benzyloxy)phenyl]-N′-ethylurea (6.3 g, 23.30 mmol) was dissolved in ethanol (150 mL). 10% Palladium on carbon (0.6 g) was added and the mixture shaken overnight under 50 psi hydrogen on a Parr apparatus. The solution was filtered through a Celite pad, the residue washed with ethanol and the solvent removed in vacuo to yield the title compound (3.84 g, 21.2 mmol).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06605618B2 |
| Source dataset | uspto-grants-2003_08 |
| ORD ID | ord-30ef377ce3df48559d82320135d9bdd6 |
| Source note | uspto-grants-2003_08 |