HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 396094Generated: October 30, 2026
HCID 22713353, compound → HCID 22713410, compound
https://huagongshe.com/reaction/396094
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | HCID 22713353 | HCID 22713353 | — |
| Solvent | Formic Acid | HCID 284 | — |
| Product | HCID 22713410 | HCID 22713410 | 79.5% |
Reaction Steps
8-[4-(1-Piperidinylsulfonyl)phenyl]-1,4-dioxa-8-azaspiro[4.5]decane (1.0 g, 2.73 mmol) was dissolved in formic acid and heated at 60° C. for 1 hour. The solvent was removed in vacuo and the residue crystallized from ethanol to give the title compound (0.70 g, 2.17 mmol).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US06605618B2 |
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| Source dataset | uspto-grants-2003_08 |
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| ORD ID | ord-7b54b6aba89d466193253aa5632b1da1 |
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| Source note | uspto-grants-2003_08 |
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