HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 21353733, compound → HCID 23003081, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 21353733 | HCID 21353733 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 23003081 | HCID 23003081 | 95% |
Reaction Steps
Analogously to the procedure of Example X, starting from 1.44 g (4.45 mmol) of 1-[5-(benzyloxy)-2-nitrophenyl]-2-hexin-1-one with 0.20 g of palladium/carbon (10%) in 50 ml of ethanol under hydrogen, after 3 h 874 mg (95%) of 1-(2-amino-5-hydroxyphenyl)-1-hexanone are obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06608049B2 |
| Source dataset | uspto-grants-2003_08 |
| ORD ID | ord-1eb1bc36756d43368e825aa70359a4e7 |
| Source note | uspto-grants-2003_08 |