HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 86586631, compound → HCID 23003083, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 86586631 | HCID 86586631 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 23003083 | HCID 23003083 | 97% |
Reaction Steps
Analogously to the procedure of Example X, starting from 1.31 g (4.42 mmol) of E/Z-1-[5-(benzyloxy)-2-nitrophenyl]-2-buten-1-one with 0.17 g of palladium/carbon (10%) in 30 ml of ethanol under hydrogen, after 3 h 770 mg (97%) of 1-(2-amino-5-hydroxyphenyl)-1-butanone are obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06608049B2 |
| Source dataset | uspto-grants-2003_08 |
| ORD ID | ord-5bf06409da3c4a4aa153deef1b31876d |
| Source note | uspto-grants-2003_08 |