HuagongsheHuagongshe Chemistry Print Report · For research reference only
3,5-dimethylpyridine-2-carbonitrile → HCID 23003411, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3,5-dimethylpyridine-2-carbonitrile | HCID 8167269 | — |
| Reactant | 1-(4-Chloro-pyridin-2-yl)-ethanone | HCID 13011986 | — |
| Reactant | HCID 23003480 | HCID 23003480 | — |
| Product | HCID 23003411 | HCID 23003411 | — |
Reaction Steps
The title compound was prepared from 3,5-dimethylpyridinecarbonitrile (K. Takahashi et al., J. Heterocycl. Chem., 1978, 15, 893) according to the procedure for preparing 2-acetyl-4-chloropyridine described in Example 33. 1H-NMR (CDCl3) δ: 8.32 (1H, s), 7.37 (1H, s), 2.69 (3H, s), 2.56 (3H, s), 2.36 (3H, s). 2-Bromoacetyl-3,5-dimethylpyridine hydrobromide:
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06608070B1 |
| Source dataset | uspto-grants-2003_08 |
| ORD ID | ord-daded8e4a70c45fe81c44b5c5c71b4ad |
| Source note | uspto-grants-2003_08 |