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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 39653Generated: October 28, 2026

Ethyl Acetate → 3,5-Dimethoxy-4-methyl-benzoic acid N-(1-tert-butyl-butyl)-N'-(2-ethyl-3-methoxy-benzoyl)-hydrazide

https://huagongshe.com/reaction/39653

Reaction equation

Participants

RoleNameHCIDCharge
ReactantEthyl AcetateHCID 8857—
ReactantHCID 66764497HCID 66764497—
SolventHexaneHCID 8058—
Product3,5-Dimethoxy-4-methyl-benzoic acid N-(1-tert-butyl-butyl)-N'-(2-ethyl-3-methoxy-benzoyl)-hydrazideHCID 66764384—

Reaction Steps

RG-115852, 3,5-dimethoxy-4-methyl-benzoic acid N-(1-tert-butyl-pentyl)-N′-(3-methoxy-2-methyl-benzoyl)-hydrazide. 1H NMR (CDCl3, 500 MHz), δ (ppm): 7.05 (t, 1H), 7.0 (s, 1H), 6.85 (d, 1H), 6.65 (s, 2H), 6.25 (d, 1H), 4.7 (d, 1H), 3.89 (s, 3H), 3.78 (s, 6H), 2.10 (s, 3H), 1.86 (s, 3H), 1.3-1.6 (br m, 6H), 1.06, 0.99 (2s, 9H), 0.94 (t, 3H); TLC Rf=0.55 (1:1 ethyl acetate:hexane).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08524948B2
Source datasetuspto-grants-2013_09
ORD IDord-0ac575e2a1c8475b819f398fe580de22
Source noteuspto-grants-2013_09