HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → HCID 70032616, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | 4,4-bis(4-methoxyphenyl)piperidine | HCID 11300958 | — |
| Reactant | HCID 12425358 | HCID 12425358 | — |
| Product | HCID 70032616 | HCID 70032616 | — |
Reaction Steps
A mixture of benzyl butyrylacetate (22.0 g, 0.10 mol) and 10 g of 4 A molecular sieves was treated with ammonia gas which was bubbled through the mixture for 38 hrs at 50° C. After filtration, benzyl 3-amino-2-hexenoate was obtained as a yellowish oil (21 g, 95%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06608086B2 |
| Source dataset | uspto-grants-2003_08 |
| ORD ID | ord-e555c6d308a94111b4779d599300eb06 |
| Source note | uspto-grants-2003_08 |