HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dichloromethane → HCID 18172447, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dichloromethane | HCID 6344 | — |
| Reactant | 1-(4-Chlorophenyl)-6-methoxy-2-phenyl-1,2,3,4-tetrahydroisoquinoline | HCID 3024621 | — |
| Solvent | Dichloromethane methanol | HCID 21226129 | — |
| Product | HCID 18172447 | HCID 18172447 | — |
Reaction Steps
The title compound was prepared by analogy to Example 48 except that 1-(4-chloro-phenyl)-6-methoxy-2-phenyl-1,2,3,4-tetrahydroisoquinoline was used instead of 6-methoxy-1-(4-methoxy-phenyl)-2-phenyl-1,2,3,4-tetrahydroisoquinoline, and neat CH2Cl2 to 10% MeOH/CH2Cl2 was used as eluent for flash chromatography purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06608203B2 |
| Source dataset | uspto-grants-2003_08 |
| ORD ID | ord-5796a6885d4a49c798dd8693a6a3383d |
| Source note | uspto-grants-2003_08 |