HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dichloromethane → HCID 18172462, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dichloromethane | HCID 6344 | — |
| Reactant | HCID 18172408 | HCID 18172408 | — |
| Solvent | Dichloromethane methanol | HCID 21226129 | — |
| Product | HCID 18172462 | HCID 18172462 | — |
Reaction Steps
The title compound was prepared by analogy to Preparation 65 except that 4-iodo-N-[2-(3-methoxy-phenyl)-ethyl]-N-phenyl-benzamide was used instead of 4-methoxy-N-[2-(3-methoxy-phenyl)-ethyl]-N-phenyl-benzamide, and the final residue was subjected to flash chromatography using a gradient from neat CH2Cl2 to CH2Cl2:MeOH 60:1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06608203B2 |
| Source dataset | uspto-grants-2003_08 |
| ORD ID | ord-133f96c801454927ab7d476cd4baa4ca |
| Source note | uspto-grants-2003_08 |