Monoepoxycyclododecadiene → Cyclododecanol

HRID 397174Notes

Reaction equation

HRID 397174 reaction equation
[O:1]1[C:3]2[CH:4]=[CH:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][C:2]1=2>[Pd]>[CH:2]1([OH:1])[CH2:13][CH2:12][CH2:11][CH2:10][CH2:9][CH2:8][CH2:7][CH2:6][CH2:5][CH2:4][CH2:3]1

Participants

3

Reactant 1

HCID 54352584Monoepoxycyclododecadiene

Product 1

HCID 15595CyclododecanolYield 5%

Reagents, catalysts & solvents 1

HCID 23938PalladiumCatalyst

Procedure

Further, in a Drafted Report, page 68, of the 24th “Progress in Reaction and Synthesis” Sympodium, Nov. 5 to 6, 1998, a hydrogenation reaction of an epoxycyclododecadiene in the presence of a palladium catalyst carried on a carbon material is reported. In this case, the target cyclododecanol was produced at a yield of 5%.

Workup

  1. customFurther, in a Drafted Report, page 68, of the 24th “Progress in Reaction and Synthesis” Sympodium, Nov

Sources & evidence

ORD record
ord-1a0df10e5d4148f183d43a4c9888d7f1
Source dataset
uspto-grants-2003_08
Patent number
US06608235B1

Reaction notes

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