Propylene → HCID 14993997, compound

HRID 397177Notes

Reaction equation

HRID 397177 reaction equation
[Cl:1][CH2:2][CH2:3][C:4](Cl)=[O:5].[Al+3].[Cl-:8].[Cl-].[Cl-].[CH2:11]=[CH:12][CH3:13]>C(Cl)Cl>[Cl:1][CH2:2][CH2:3][C:4]([CH2:11][CH:12]([CH3:13])[Cl:8])=[O:5]

Participants

5

Reactant 3

HCID 8252PropyleneHCID 693643-Chloropropionyl chlorideHCID 6451240Aluminum(III) Chloride

Product 1

HCID 14993997HCID 14993997, compound

Reagents, catalysts & solvents 1

HCID 6344DichloromethaneSolvent

Procedure

At room temperature, 507.88 g of 3-chloropropionyl chloride are added dropwise over a period of 15 minutes to 758.08 g (5.6 mol) of AlCl3 in 560 ml of methylene chloride, and 189 g (4.5 mol) of propylene are introduced into this mixture at approximately 28 to 30° C. over a period of approximately 3 hours.

Workup

  1. additionare introduced into this mixture at approximately 28 to 30° C. over a period of approximately 3 hours

Sources & evidence

ORD record
ord-db6de1ea7de249508a00b0b0937ca0be
Source dataset
uspto-grants-2003_08
Patent number
US06608211B1

Reaction notes

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