HuagongsheHuagongshe Chemistry Print Report · For research reference only
Propylene → HCID 14993997, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Propylene | HCID 8252 | — |
| Reactant | 3-Chloropropionyl chloride | HCID 69364 | — |
| Reactant | Aluminum(III) Chloride | HCID 6451240 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 14993997 | HCID 14993997 | — |
Reaction Steps
At room temperature, 507.88 g of 3-chloropropionyl chloride are added dropwise over a period of 15 minutes to 758.08 g (5.6 mol) of AlCl3 in 560 ml of methylene chloride, and 189 g (4.5 mol) of propylene are introduced into this mixture at approximately 28 to 30° C. over a period of approximately 3 hours.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06608211B1 |
| Source dataset | uspto-grants-2003_08 |
| ORD ID | ord-db6de1ea7de249508a00b0b0937ca0be |
| Source note | uspto-grants-2003_08 |