HuagongsheHuagongshe Chemistry Print Report · For research reference only
Butylamine → HCID 70025618, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Butylamine | HCID 8007 | — |
| Reactant | HCID 12114669 | HCID 12114669 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 70025618 | HCID 70025618 | — |
Reaction Steps
A mixture of (4-methoxyphenyl)-(4-(2,3-epoxypropyloxy)phenyl)-1,2,3,4-tetrahydronaphth-1-yl-methane (400 mg, 0.01 mol), n-butyl amine (1.0 ml, 0.01 mol) and ethanol (10 ml) was refluxed for 8 hrs. Ethanol was distilled off and the residue was passed through basic alumina using benzene:ethyl acetate as the eluent. The solvent was distilled off yielding the required product. Yield 230 mg (48.93%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06610705B1 |
| Source dataset | uspto-grants-2003_08 |
| ORD ID | ord-ac0b4bfc357d46559060f3ffcbb07281 |
| Source note | uspto-grants-2003_08 |