HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → Benzyl 3-[(chlorosulfonyl)methyl]piperidine-1-carboxylate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 1-[(Benzyloxy)carbonyl]-3-piperidylmethanesulfonic acid | HCID 54551842 | — |
| Product | Benzyl 3-[(chlorosulfonyl)methyl]piperidine-1-carboxylate | HCID 23000683 | — |
Reaction Steps
The title compound was prepared by the method of Preparation 58 from 1-[(benzyloxy)carbonyl]-3-piperidylmethanesulfonic acid [see Preparation 61]and thionyl chloride to afford benzyl 3-[(chlorosulfonyl)methyl]-1-piperidinecarboxylate as an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06610707B1 |
| Source dataset | uspto-grants-2003_08 |
| ORD ID | ord-d7f4afb515d04e3eb6d16f19603e12fc |
| Source note | uspto-grants-2003_08 |