Sodium Sulfite → Sodium cyclopentylmethanesulfonate
Reaction equation
Br[CH2:2][CH:3]1[CH2:7][CH2:6][CH2:5][CH2:4]1.[S:8]([O-:11])([O-:10])=[O:9].[Na+:12].[Na+]>>[CH:3]1([CH2:2][S:8]([O-:11])(=[O:10])=[O:9])[CH2:7][CH2:6][CH2:5][CH2:4]1.[Na+:12]Participants
3
Procedure
The subtitle compound was prepared by the method of Preparation 61 from 1-(bromomethyl)cyclopentane [Preparation 63] and sodium sulphite. The crude product was purified by recrystallisation from water to afford sodium cyclopentylmethanesulfonate as a white solid.
Workup
- customThe crude product was purified by recrystallisation from water
Sources & evidence
- ORD record
- ord-510a1b58e9e24f5881de135df329434a
- Source dataset
- uspto-grants-2003_08
- Patent number
- US06610707B1
Reaction notes
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