Carbon tetrabromide → (Bromomethyl)cycloheptane

HRID 397683Notes

Reaction equation

HRID 397683 reaction equation
[CH:1]1([CH2:8]O)[CH2:7][CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1.C(Br)(Br)(Br)[Br:11]>>[Br:11][CH2:8][CH:1]1[CH2:7][CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1

Participants

3

Reactant 2

HCID 11205Carbon tetrabromideHCID 78193Cycloheptanemethanol

Product 1

HCID 23000753(Bromomethyl)cycloheptane

Procedure

The subtitle compound was prepared by the method of Preparation 9 from cycloheptylmethanol and carbon tetrabromide. The crude product was purified by fractional distillation, b.pt. 115° C.-120° C. @ 30mmHg to afford 1-(bromomethyl)cycloheptane as an oil.

Workup

  1. distillationThe crude product was purified by fractional distillation, b.pt. 115° C.-120° C.

Sources & evidence

ORD record
ord-082a997b385e4a4ea28cd2683bd2593d
Source dataset
uspto-grants-2003_08
Patent number
US06610707B1

Reaction notes

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