HuagongsheHuagongshe Chemistry Print Report · For research reference only
Carbon tetrabromide → (Bromomethyl)cycloheptane
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Carbon tetrabromide | HCID 11205 | — |
| Reactant | Cycloheptanemethanol | HCID 78193 | — |
| Product | (Bromomethyl)cycloheptane | HCID 23000753 | — |
Reaction Steps
The subtitle compound was prepared by the method of Preparation 9 from cycloheptylmethanol and carbon tetrabromide. The crude product was purified by fractional distillation, b.pt. 115° C.-120° C. @ 30mmHg to afford 1-(bromomethyl)cycloheptane as an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06610707B1 |
| Source dataset | uspto-grants-2003_08 |
| ORD ID | ord-082a997b385e4a4ea28cd2683bd2593d |
| Source note | uspto-grants-2003_08 |