Sodium Sulfite → Sodium cycloheptylmethanesulfonate

HRID 397684Notes

Reaction equation

HRID 397684 reaction equation
Br[CH2:2][CH:3]1[CH2:9][CH2:8][CH2:7][CH2:6][CH2:5][CH2:4]1.[S:10]([O-:13])([O-:12])=[O:11].[Na+:14].[Na+]>>[CH:3]1([CH2:2][S:10]([O-:13])(=[O:12])=[O:11])[CH2:9][CH2:8][CH2:7][CH2:6][CH2:5][CH2:4]1.[Na+:14]

Participants

3

Reactant 2

HCID 24437Sodium SulfiteHCID 23000753(Bromomethyl)cycloheptane

Product 1

HCID 23670189Sodium cycloheptylmethanesulfonate

Procedure

The subtitle compound was prepared by the method of Preparation 61 from 1-(bromomethyl)cycloheptane [Preparation 66] and sodium sulfite. The crude product was purified by recrystallisation from water to afford sodium cycloheptylmethanesulfonate as a white solid.

Workup

  1. customThe crude product was purified by recrystallisation from water

Sources & evidence

ORD record
ord-492a299d80e24777a8278b20b341f235
Source dataset
uspto-grants-2003_08
Patent number
US06610707B1

Reaction notes

Loading…