참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Hydrochloric Acid | HCID 313 | — |
| 반응물 | Diethyl Ether | HCID 3283 | — |
| 반응물 | Cyclopropanecarbonitrile | HCID 79637 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | Ethyl cyclopropanecarboximidate hydrochloride | HCID 20026660 | 59% |
반응 단계
A steady stream of HCl gas was slowly passed through a solution of cyclopropancarbonitril (25 g, 373 mmol) in EtOH (17.2 ml). After 15 h the reaction mixture was cooled to 0° C. and diethylether was added dropwise. The precipitated title compound was filtered and obtained as a colourless crystalline material (32.9 g, 220 mmol, 59%). MS: m/e=112.2 (M−H).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US06610723B2 |
|---|
| 출처 데이터셋 | uspto-grants-2003_08 |
|---|
| ORD ID | ord-82b83684b24e4704b279c0b7d2caca4b |
|---|
| 출처 메모 | uspto-grants-2003_08 |
|---|
