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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 397974Generated: October 28, 2026

Hydrochloric Acid → HCID 9939091, compound

https://huagongshe.com/reaction/397974

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHydrochloric AcidHCID 313—
ReactantWaterHCID 962—
ReactantSodium HydroxideHCID 14798—
ReactantHCID 9831339HCID 9831339—
SolventMethanolHCID 887—
ProductHCID 9939091HCID 9939091—

Reaction Steps

0.25 g (0.37 mmol) of 2-cyanoethyl 4-(3-chlorophenyl)-6-(2-cyclohexylethoxymethyl)-5-(3,3-diphenylpropylcarbamoyl)-2-methyl-1,4-dihydropyridine-3-carboxylate was dissolved in 5 ml of methanol. 0.73 ml of 1 N aqueous sodium hydroxide solution was added to the obtained solution, and they were stirred at room temperature for 2 hours. 1 N hydrochloric acid and water were added to the reaction mixture. The precipitates thus formed were taken by the filtration and dried under reduced pressure to obtain the title compound.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06610717B2
Source datasetuspto-grants-2003_08
ORD IDord-487955a6ab7f49778aea24d446ee5bfa
Source noteuspto-grants-2003_08