Cyclopentylamine → HCID 70021884, compound

Participants

Reaction Steps

Intermediate 17 (0.048 g), cyclopentylamine (0.06 ml) in DMSO (0.05 ml) were heated in a sealed vial (eg Reacti vial™) at 90° C. for 20 hrs. The crude material was purified by Autoprep HPLC, solvent was removed in vacuo and the residue freeze-dried to give the title compound as a pale yellow solid (0.006 g) LC/MS system A Rt=2.2 min, m/z=403(MH+)

Provenance & Evidence