Hydrogen Bromide → HCID 23001313, compound

Participants

Reaction Steps

The sulfone from Step B (1.32 g, 3.67 mmol) in acetic acid (2 mL) and 48% HBr (2 mL) was heated at 100° C. for 72 hours. The reaction mixture was concentrated and the solid residue triturated with ether (200 mL) to produce the title compound as a grey solid.

Provenance & Evidence