HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 23001302, compound → HCID 70025062, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 23001302 | HCID 23001302 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 70025062 | HCID 70025062 | — |
Reaction Steps
A solution of azide from Step C (57.0 mg, 0.134 mmol) and 10% palladium on carbon (57.0 mg) in methanol (5 mL) was placed under a hydrogen atmosphere (1 atm) for 16 hours. The reaction mixture was filtered through a Celite pad and concentrated in vacuo to provide the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06610722B2 |
| Source dataset | uspto-grants-2003_08 |
| ORD ID | ord-3303d2cf3cf74e7abdcf44f85f387153 |
| Source note | uspto-grants-2003_08 |