HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Bisulfate → HCID 23002371, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Bisulfate | HCID 516919 | — |
| Reactant | Sodium Nitrite | HCID 23668193 | — |
| Reactant | HCID 43627497 | HCID 43627497 | — |
| Product | HCID 23002371 | HCID 23002371 | 1,174.2% |
Reaction Steps
2-amino-N-methyl-N-methoxyphenylsulfonamide [Xn=2-SO2N(OCH3)CH3 in Compound (XXV)] (5.4 g, 25 mmol) was diazotized with sodium nitrite (2.07 g, 25×1.2 mmol) and the resultant diazonium compound was allowed to react with sodium hydrogen sulfate (7.28 g, 25×2.8 mmol) to obtain 3.95 g (percent yield: 56.37%) of 2-[(N-methyl-N-methoxyamino)sulfonyl] phenylsulfonamide [Compound (III-18)].
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06610853B1 |
| Source dataset | uspto-grants-2003_08 |
| ORD ID | ord-75e04276fac44a27a2454d2726e5ff4a |
| Source note | uspto-grants-2003_08 |