HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylformamide → HCID 54259741, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylformamide | HCID 6228 | — |
| Reactant | 4-Methyl-5-nitropyridine-2-carbonitrile | HCID 23000171 | — |
| Product | HCID 54259741 | HCID 54259741 | — |
Reaction Steps
A stirred solution of 2-cyano-4-methyl-5-nitropyridine (2.48 g, 15.2 mmol) in DMF (10 mL) and DMF-dimethylacetal (2.7 mL, 20 mmol) was heated to 90° C. for two h. The solution was cooled and evaporated in vacuo to give the title compound as a deep red solid:
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06610692B1 |
| Source dataset | uspto-grants-2003_08 |
| ORD ID | ord-29dd05ebc4b9480cae3bc0def21340b0 |
| Source note | uspto-grants-2003_08 |