HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 23000277, compound → 4-Methyl-1H-pyrrolo[2,3-b]pyridine-5-carbonitrile
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 23000277 | HCID 23000277 | — |
| Catalyst | HCID 178418406 | HCID 178418406 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | 4-Methyl-1H-pyrrolo[2,3-b]pyridine-5-carbonitrile | HCID 23000237 | — |
Reaction Steps
A mixture of 5-cyano-4-methyl-7-azaindoline (52 mg, 0.33 mmol) and manganese dioxide (130 mg, 1.5 mmol) in chloroform (10 mL) was stirred for 16 h and then was filtered through celite, washing through with chloroform followed by methanol. The filtrate was evaporated in vacuo to give the title compound as a tan solid:
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06610692B1 |
| Source dataset | uspto-grants-2003_08 |
| ORD ID | ord-dd8fbfc54c8a4cd68855d8c458a08a9c |
| Source note | uspto-grants-2003_08 |