HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 23000187, compound → HCID 54725781, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 23000187 | HCID 23000187 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 54725781 | HCID 54725781 | — |
Reaction Steps
A mixture of 3-benzyloxy-4-diisobutylaminocarbonyl-6-methyl-1-tert-butyloxycarbonylmethyl-2-pyridinone from step 4 above (0.80 g) and 10% Pd on carbon (180 mg) in ethanol (40 mL) was shaken on a Parr apparatus under an atmosphere of hydrogen (50 psi) for 18 h. The catalyst was removed by filtration and the filtrate solvents were removed in vacuo to give the title compound (0.608 g;
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06610692B1 |
| Source dataset | uspto-grants-2003_08 |
| ORD ID | ord-ae3967df5b1c4f24b3022373f7fa0d07 |
| Source note | uspto-grants-2003_08 |