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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 398374Generated: October 30, 2026

HCID 23000187, compound → HCID 54725781, compound

https://huagongshe.com/reaction/398374

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 23000187HCID 23000187—
CatalystPalladiumHCID 23938—
SolventEthanolHCID 702—
ProductHCID 54725781HCID 54725781—

Reaction Steps

A mixture of 3-benzyloxy-4-diisobutylaminocarbonyl-6-methyl-1-tert-butyloxycarbonylmethyl-2-pyridinone from step 4 above (0.80 g) and 10% Pd on carbon (180 mg) in ethanol (40 mL) was shaken on a Parr apparatus under an atmosphere of hydrogen (50 psi) for 18 h. The catalyst was removed by filtration and the filtrate solvents were removed in vacuo to give the title compound (0.608 g;

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06610692B1
Source datasetuspto-grants-2003_08
ORD IDord-ae3967df5b1c4f24b3022373f7fa0d07
Source noteuspto-grants-2003_08