Isoamylamine → HCID 86753200, compound

HRID 399099Notes

Reaction equation

HRID 399099 reaction equation
[CH2:1]([NH2:6])[CH2:2][CH:3]([CH3:5])[CH3:4].[CH2:7]([NH:9][C:10]([NH:12][C@H:13]([C:21]([OH:23])=[O:22])[CH2:14][C:15]1[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=1)=[O:11])[CH3:8].[NH2:24][C@H:25]([C:29]([OH:31])=[O:30])[CH:26]([CH3:28])[CH3:27].[NH2:32][C@H:33]([C:35](O)=[O:36])[CH3:34]>>[CH2:7]([NH:9][C:10]([NH:12][C@H:13]([C:21]([OH:23])=[O:22])[CH2:14][C:15]1[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=1)=[O:11])[CH3:8].[NH2:24][C@H:25]([C:29]([OH:31])=[O:30])[CH:26]([CH3:28])[CH3:27].[CH2:1]([NH:6][C:35](=[O:36])[C@H:33]([CH3:34])[NH2:32])[CH2:2][CH:3]([CH3:5])[CH3:4]

Participants

3

Reactant 2

HCID 7894IsoamylamineHCID 67651764HCID 67651764, compound

Product 1

HCID 86753200HCID 86753200, compound

Procedure

The compound was prepared by the standard resin cleavage procedure for amines of Example 57, Step 1, using isoamyl amine (1.5 mL) and N-ethylcarbamoyl-phenylalanine-valine-alanine-® Pam resin (151 mg, Preparation 5). Purification of the product was effected by using the purification procedure of Example 57, Step 2, affording the product as a white solid.

Workup

  1. customPurification of the product
  2. customthe purification procedure of Example 57, Step 2

Sources & evidence

ORD record
ord-41038865a1a2489a801398326d25899a
Source dataset
uspto-grants-1998_10
Patent number
US05817757

Reaction notes

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