HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 18393861, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | HCID 21835122 | HCID 21835122 | — |
| Reactant | HCID 86753201 | HCID 86753201 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 18393861 | HCID 18393861 | — |
Reaction Steps
A solution of 18.4 g (0.108 moles) of N-(3-chlorophenyl)-ethanediamine (J. Med. Chem., 9, 858-860 (1966)), 19.3 ml (0.119 moles) of (S)-methanesulfonyl-lactic acid ethyl ester and 22.8 ml (0.163 moles) of triethylamine in 200 ml of toluene was boiled and refluxed overnight.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05817815 |
| Source dataset | uspto-grants-1998_10 |
| ORD ID | ord-7a973375b9d645b48d650671ec42d041 |
| Source note | uspto-grants-1998_10 |