HuagongsheHuagongshe Chemistry Print Report · For research reference only
Stannous Chloride → HCID 85766638, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Stannous Chloride | HCID 24479 | — |
| Reactant | Acetylacetone | HCID 31261 | — |
| Reactant | 3-Phenylprop-2-enoyl chloride | HCID 66023 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 85766638 | HCID 85766638 | 101.6% |
Reaction Steps
The procedure was analogous to Example 6. 50 g (0.26 mol) of tin(II) chloride and 25.6 g (0.26 mol) of acetylacetone was reacted with 44 g (0.26 mol) of cinnamoyl chloride in 150 ml of diethyl ether to give a quantitative yield of 81.4 g of 1-methylbut-1-en-3-onyltin trichloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05817851 |
| Source dataset | uspto-grants-1998_10 |
| ORD ID | ord-632b97e2168f4eac891e25124716dada |
| Source note | uspto-grants-1998_10 |