HuagongsheHuagongshe Chemistry Print Report · For research reference only
Butylamine → N-butyl-2-methylaniline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Butylamine | HCID 8007 | — |
| Reactant | o-Tolyl Trifluoromethanesulfonate | HCID 572025 | — |
| Product | N-butyl-2-methylaniline | HCID 11073747 | 67% |
Reaction Steps
General procedure B using 55.1 mg (0.229 mmol) of o-tolyltriflate and 34.0 μl (0.344 mmol) of n-butylamine gave 67% yield of N-butyl-2-methylaniline after silica gel chromatograph using 5% ethyl acetate in hexanes.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05817877 |
| Source dataset | uspto-grants-1998_10 |
| ORD ID | ord-fdcf88cbec6c46eeba2949b035418134 |
| Source note | uspto-grants-1998_10 |