HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Pentyne → HCID 11137342, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Pentyne | HCID 12309 | — |
| Reactant | 2-Bromothiophene | HCID 13851 | — |
| Reactant | Butyllithium | HCID 178418339 | — |
| Catalyst | Zincchloride | HCID 3007855 | — |
| Product | HCID 11137342 | HCID 11137342 | — |
Reaction Steps
Quantities: pent-1-yne (6.80 g, 0.10 mol), n-butyllithium (10.0 ml, 10.0M in hexane, 0.044 mol), zinc chloride (13.60 g, 0.10 mol), 2-bromothiophene (16.00 g, 0.098 mol), tetrakis (triphenylphosphine)palladium(O) (3.40 g 2.94 mol).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05820781 |
| Source dataset | uspto-grants-1998_10 |
| ORD ID | ord-62deb6676c1f4f969ce22e4eaded88e9 |
| Source note | uspto-grants-1998_10 |