HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 86753214, compound → HCID 18665857, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 86753214 | HCID 86753214 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 18665857 | HCID 18665857 | — |
Reaction Steps
A solution of 9-2 (612 mg, 1.65 mmol) in ethyl acetate (50 ml) was cooled to -5° and anhydrous HCl was bubbled in for 30 min. The reaction was concentrated and the product isolated by filtration to give 9-3 as a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05821241 |
| Source dataset | uspto-grants-1998_10 |
| ORD ID | ord-ee56789f8e164366bf553197365c0992 |
| Source note | uspto-grants-1998_10 |