HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Chloro-1-fluoro-4-nitrobenzene → 2-Chloro-4-nitrophenyl 2-thienyl sulphide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Chloro-1-fluoro-4-nitrobenzene | HCID 67688 | — |
| Reactant | 2-Thiophenethiol | HCID 522674 | — |
| Product | 2-Chloro-4-nitrophenyl 2-thienyl sulphide | HCID 18967579 | 32% |
Reaction Steps
Using an analogous procedure to that described in the first paragraph of the portion of Example 8 which is concerned with the preparation of starting materials, 3-chloro-4-fluoronitrobenzene was reacted with 2-thiophenethiol to give 2-chloro-4-nitrophenyl 2-thienyl sulphide in 32% yield.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05821246 |
| Source dataset | uspto-grants-1998_10 |
| ORD ID | ord-f68f3c549d444d70bd946afdde28bb94 |
| Source note | uspto-grants-1998_10 |