HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 18967863, compound → HCID 18967860, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 18967863 | HCID 18967863 | — |
| Catalyst | Nickel | HCID 935 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 18967860 | HCID 18967860 | — |
Reaction Steps
A solution of 1 g of 2-(4-nitrophenyl)-2-(1,3-dihydro-1,3-dioxoisoindol-5-yloxy)-N-(4-tertbutylphenylsulfonyl)acetamide in 25 ml of methanol is hydrogenated to completion at normal pressure and 20° on 1 g of Raney nickel. The mixture is filtered, the solvent is removed and 2-(4-aminophenyl)-2-(1,3-dihydro-1,3-dioxoisoindol-5-yloxy)-N-(4-tert-butylphenylsulfonyl)acetamide is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05821256 |
| Source dataset | uspto-grants-1998_10 |
| ORD ID | ord-6f710e43cd03414db2e55197c9f4a0f2 |
| Source note | uspto-grants-1998_10 |