HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Azabicyclo[2.2.2]octane-4-carbonitrile → Quinuclidin-4-ylmethanamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Azabicyclo[2.2.2]octane-4-carbonitrile | HCID 141292 | — |
| Solvent | Dichloromethane methanol | HCID 21226129 | — |
| Product | Quinuclidin-4-ylmethanamine | HCID 22056669 | — |
Reaction Steps
Colourless oil; Rf : 0.3 (trace of tailing; alumina; methylene chloride/methanol=7:3); Mass spectrum: M+=140; Prepared from 4-cyanoquinuclidine (see Example 3 of EP-A-0,213,337).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05821240 |
| Source dataset | uspto-grants-1998_10 |
| ORD ID | ord-939eed98b7bf40c9a1e9354970f719ef |
| Source note | uspto-grants-1998_10 |