HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanesulfonyl chloride → HCID 18967420, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanesulfonyl chloride | HCID 31297 | — |
| Reactant | HCID 18967290 | HCID 18967290 | — |
| Solvent | Triethylamine | HCID 8471 | — |
| Product | HCID 18967420 | HCID 18967420 | — |
Reaction Steps
Prepared from Compound 153 in Example 1 by reaction with methanesulphonyl chloride and triethylamine. Melting point: 225°-227° C.; Rf : 0.53 (alumina; petroleum ether/ethyl acetate/methanol=10:10:1); Calculated: C 48.97 H 4.54 N 21.04; Found: 49.07 4.59 20.75
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05821240 |
| Source dataset | uspto-grants-1998_10 |
| ORD ID | ord-4db20fec0bfa4a0bad728fcc7e35f418 |
| Source note | uspto-grants-1998_10 |