HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl Bromide → HCID 18944861, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl Bromide | HCID 6332 | — |
| Reactant | Ethyl 2-methyl-3-oxo-3,4-dihydro-2H-1,4-benzoxazine-2-carboxylate | HCID 3378326 | — |
| Product | HCID 18944861 | HCID 18944861 | — |
Reaction Steps
The title compound was prepared from ethyl-3,4-dihydro-2-methyl-3-oxo-2H-1,4-benzoxazine-2-carboxylate and ethyl bromide according to the procedure described in Example 16. The title product was a viscous oil, which was purified by column chromatography (silica gel; dichloromethane/methanol 100:1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05824652 |
| Source dataset | uspto-grants-1998_10 |
| ORD ID | ord-76ab090f3d874a6bab89c6a355165081 |
| Source note | uspto-grants-1998_10 |