HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 54158441, compound → HCID 54416739, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 54158441 | HCID 54158441 | — |
| Solvent | Hydrochloric Acid | HCID 313 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 54416739 | HCID 54416739 | — |
Reaction Steps
[1-Hydroxy-2-(2-(acetylthio)cyclohexyl)ethylidene]bis[phosphonic acid] is heated at reflux in concentrated hydrochloric acid for 7 hours. The reaction is concentrated under reduced pressure and the solid residue is triturated in ethanol. The product is obtained by recrystallization the crude solid in ethanol and water.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05824661 |
| Source dataset | uspto-grants-1998_10 |
| ORD ID | ord-a87cb3130d934237aad5fdd6538aa0ad |
| Source note | uspto-grants-1998_10 |