Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Jineol → 3,8-Dimethoxy quinoline
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Jineol | HCID 177338 | — |
| 반응물 | Diazomethane diethylether | HCID 21186548 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | 3,8-Dimethoxy quinoline | HCID 10583798 | 80% |
반응 단계
Jineol of 4.5 mg was dissolved in 2 ml of ethanol, and diazomethane ether solution was slowly dropped to the solution. After the excess of diazomethane and solvent was removed by purging with nitrogen gas, the solution was purified by silicagel chromatography to give 4.2 mg of 3,8-dimethoxy quinoline with 80% yield.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05824689 |
| 출처 데이터셋 | uspto-grants-1998_10 |
| ORD ID | ord-a3d35d944aca43608a8e9c356519b602 |
| 출처 메모 | uspto-grants-1998_10 |