Diisopropyl Ether → HCID 18945281, compound

Participants

Reaction Steps

4N-Hydrogen chloride-dioxane (3.0 ml) was added to a mixture of 2-[3-(1H-tetrazol-1-yl)benzoyl]guanidine (1.4 g) in methanol (30 ml) and the mixture was stirred for 1 hour at ambient temperature. To the mixture was added diisopropyl ether (30 ml) and the precipitate was collected by filtration. The precipitate was recrystallized from methanol to give 2-[3-(1H-tetrazol-1-yl)benzoyl]guanidine hydrochloride (1.05 g).

Provenance & Evidence