HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanesulfonic Acid → HCID 86753234, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanesulfonic Acid | HCID 6395 | — |
| Reactant | HCID 18945260 | HCID 18945260 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 86753234 | HCID 86753234 | — |
Reaction Steps
Methanesulfonic acid (0.5 ml) was added to a solution of 2-[3-(2-cyanopyrrol-1-yl)-5-(diaminomethyleneaminocarbonyl) benzoyl]guanidine (0.8 g) in methanol (16 ml) and the whole was stirred for 1 hour at ambient temperature. The isolated precipitate was collected by filtration and recrystallized from water to give 2-[3-(2-cyanopyrrol-1-yl) -5-(diaminomethyleneaminocarbonyl)benzoyl]guanidine dimethanesulfonate (0.65 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05824691 |
| Source dataset | uspto-grants-1998_10 |
| ORD ID | ord-9e01f88bfde249f1833d15a2fd301cbc |
| Source note | uspto-grants-1998_10 |