Methyl perfluorobutyl ether → 1,1,1,2,2,3,4,5,5,5-Decafluoropentane

HRID 400083Notes

Reaction equation

HRID 400083 reaction equation
[C:1]([O:14][CH3:15])([C:4]([C:7]([C:10]([F:13])([F:12])[F:11])([F:9])[F:8])([F:6])[F:5])([F:3])[F:2]>CO.C(O)(C)C.C(O)C.CC(C)=O.CCCCCCC>[C:1]([O:14][CH3:15])([C:4]([C:7]([C:10]([F:12])([F:13])[F:11])([F:9])[F:8])([F:6])[F:5])([F:3])[F:2].[CH:4]([F:6])([C:7]([F:9])([F:8])[C:10]([F:13])([F:12])[F:11])[CH:1]([F:3])[C:10]([F:13])([F:12])[F:11]

Participants

8

Reactant 1

HCID 164514Methyl perfluorobutyl ether4×

Product 2

HCID 862401,1,1,2,2,3,4,5,5,5-DecafluoropentaneHCID 164514Methyl perfluorobutyl ether

Reagents, catalysts & solvents 5

HCID 180AcetoneSolvent2×HCID 702EthanolSolvent5×HCID 887MethanolSolvent6×HCID 3776IsopropanolSolvent4×HCID 8900HeptaneSolvent2×

Procedure

The present invention also relates to the discovery of azeotropic or azeotrope-like compositions of effective amounts of C4F9 OCH3 and methanol, ethanol, isopropanol, n-heptane, t-DCE, c-DCE, or acetone; C4F9OCH3, n-heptane and methanol, ethanol or isopropanol; C4F9OCH3, t-DCE and methanol, ethanol or isopropanol; C4F9OCH3, c-DCE and methanol or ethanol; C4F9OCH3, acetone and methanol, ethanol, or isopropanol; C4F9OCH3, HFC-43-10mee and methanol to form an azeotropic or azeotrope-like composition.

Sources & evidence

ORD record
ord-93965d65ebb34977840e74e7c4b57c5f
Source dataset
uspto-grants-1998_10
Patent number
US05827446

Reaction notes

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