HuagongsheHuagongshe Chemistry Print Report · For research reference only
Formic Acid → Methyl 3-formamidocinnamate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Formic Acid | HCID 284 | — |
| Reactant | Methyl 3-aminocinnamate | HCID 54385173 | — |
| Solvent | Water | HCID 962 | — |
| Product | Methyl 3-formamidocinnamate | HCID 54484240 | — |
Reaction Steps
193 g of methyl 3-aminocinnamate and 900 ml of formic acid were mixed and heated under reflux for 2 hours. The reaction solution was poured into water and the crystals (methyl 3-formamidocinnamate) obtained were collected by filtration. Yield: 127 g.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05827638 |
| Source dataset | uspto-grants-1998_10 |
| ORD ID | ord-544208453dae4717be0d51f4b646578f |
| Source note | uspto-grants-1998_10 |