HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,2-Diethoxyethylamine → HCID 18943443, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,2-Diethoxyethylamine | HCID 69524 | — |
| Reactant | tert-Butyl 4-oxopiperidine-1-carboxylate | HCID 735900 | — |
| Product | HCID 18943443 | HCID 18943443 | 5% |
Reaction Steps
The N-(1-tert-butyloxycarbonyl-4-piperidinyl)-N-(2,2-di-ethoxyethyl)amine [Rf : 0.48 (reversed phase silica gel; methanol/5% aqueous brine=6:4)] employed is prepared by reductive amination of 1-tert-butyloxycarbonyl-4-piperidone with aminoacetaldehyde diethyl acetal
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05827849 |
| Source dataset | uspto-grants-1998_10 |
| ORD ID | ord-ba2225c8df2545d0bd2e72a772527e62 |
| Source note | uspto-grants-1998_10 |