HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethyl Malonate → HCID 178468432, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethyl Malonate | HCID 7761 | — |
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | 1-benzyl-4-chloro-5-hydroxyiminomethyl-2,3,6,7-tetrahydro-1H-azepine | HCID 86621673 | — |
| Catalyst | copper(I) bromide | HCID 24593 | — |
| Product | HCID 178468432 | HCID 178468432 | — |
Reaction Steps
Prepared from 1-benzyl-4-chloro-5-hydroxyiminomethyl-2,3,6,7-tetrahydro-1H-azepine by reaction with diethyl malonate in the presence of sodium hydride and catalytic amounts of copper(I) bromide at 100° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05827849 |
| Source dataset | uspto-grants-1998_10 |
| ORD ID | ord-8427a90930f54a9caddc457a71ade9aa |
| Source note | uspto-grants-1998_10 |