HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-Methylbenzylamine → HCID 18944400, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-Methylbenzylamine | HCID 7669 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Levulinic Acid | HCID 11579 | — |
| Reactant | Isobutyl chloroformate | HCID 62365 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 18944400 | HCID 18944400 | 88.6% |
Reaction Steps
A! Starting from 10 g (0.086 mole) of levulinic acid, 11.8 ml (0.086 mole) of triethylamine, 11.2 ml (0.086 mole) of isobutyl chloroformate and 13.3 ml (0.103 mole) of N-methyl-benzylamine in 200 ml of acetone, and following the procedure of Example 6,B!, there were obtained 16.7 g (yield: 88%) of N-benzyl-N-methyl-4-oxo-pentanamide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05827881 |
| Source dataset | uspto-grants-1998_10 |
| ORD ID | ord-bbc053c6d9cc4676aa4324fea3fc855d |
| Source note | uspto-grants-1998_10 |