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HRID400225

反应详情

EQUATION

反应方程式

HRID 400225 的结构方程式

REACTANTS

反应物

3
结构：NCCO
HCID700

Ethanolamine

C2H7NO

结构：c1ccncc1
HCID1049

Pyridine

C5H5N

结构：ClC(c1ccccc1)(c1ccccc1)c1ccccc1
HCID6456

Trityl chloride

C19H15Cl

PRODUCTS

生成物

1
结构：OCCNC(c1ccccc1)(c1ccccc1)c1ccccc1
HCID3125608

2-(tritylamino)ethanol

C21H21NO

AUXILIARIES

试剂、催化剂与溶剂

1
结构：O
溶剂HCID962

Water

H2O

PROCEDURE

实验过程

A mixture of ethanolamine, trityl chloride and pyridine was refluxed for 15h. Water was added slowly to the cooled reaction and the precipitate collected by filtration. The crude product recrystallized from a 1:1 mixture of ethanol and water.

WORKUP

后处理

  1. temperaturewas refluxed for 15h
  2. filtrationthe precipitate collected by filtration
  3. customThe crude product recrystallized from a 1:1 mixture of ethanol and water