Hexane → (E)-4-(Benzyloxy)-2-butenyl acetate

HRID 400232Notes

Reaction equation

HRID 400232 reaction equation
[C:1]([O:4][CH2:5][CH3:6])(=[O:3])[CH3:2].S(OS([O-])(=O)=O)([O-])(=O)=O.[Ce+3].S(OS([O-])(=O)=O)([O-])(=O)=O.S(OS([O-])(=O)=O)([O-])(=O)=O.[Ce+3].[CH3:36][CH2:37][CH2:38][CH2:39][CH2:40][CH3:41]>>[C:1]([O:4][CH2:5]/[CH:6]=[CH:2]/[CH2:1][O:4][CH2:5][C:38]1[CH:37]=[CH:36][CH:41]=[CH:40][CH:39]=1)(=[O:3])[CH3:2]

Participants

4

Reactant 3

HCID 8058HexaneHCID 8857Ethyl AcetateHCID 22269528HCID 22269528, compound

Product 1

HCID 14916057(E)-4-(Benzyloxy)-2-butenyl acetate

Procedure

TLC: Rf =0.52, silica gel, 20% ethyl acetate in hexane, UV & cerium disulfate.

Sources & evidence

ORD record
ord-5dfb2d41abf14909bdba48dbbb2e205f
Source dataset
uspto-grants-1998_10
Patent number
US05827868

Reaction notes

Loading…