HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 400252Generated: October 30, 2026
HCID 22669967, compound → HCID 21841494, compound
https://huagongshe.com/reaction/400252
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | HCID 22669967 | HCID 22669967 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 21841494 | HCID 21841494 | 99.1% |
Reaction Steps
The mixture of 286 mg of the product of Stage B, 91 mg of 9.5% palladium on charcoal and 20 ml of ethyl acetate was placed under a hydrogen atmosphere and the mixture was stirred at 20° C. for 24 hours. After filtration and concentration under reduced pressure, 211 mg of the expected product were obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US05827887 |
|---|
| Source dataset | uspto-grants-1998_10 |
|---|
| ORD ID | ord-f43cb7f94ba748b5bc98ff0f1142e932 |
|---|
| Source note | uspto-grants-1998_10 |
|---|
